My experimental device:
1 ) Reactor length: 350mm, inner diameter 30mm, wall thickness 5mm. The reactor is connected with the hydrogen cylinder, the argon gas cylinder and the pressure transmitter through the pipeline.
2 ) K Type thermocouples for temperature measurement, T1 measurement of furnace temperature, T2 measurement of reactor surface temperature, room temperature measurement.
3 )Heating system using 2KW resistance wire furnace and furnace temperature control instrument.
Recording temperature and pressure data using a recorder
4) 20g micron nickel powder
2G LiAlH4
1g Lithium
The experiment was carried out according to the method of MFMP.
Unfortunately, a few days of the experiment did not detect any abnormal heat.
Please give me some guidance and advice!
What size of nickel powder? Nickel powder is prepared by what method? How to deal with it?
Thank you for your valuable suggestions, I will continue to work hard to test, and gradually released on the forum.