72 hours is WAY too long. That is not a useful calorimeter. The results will be blurred out over those same 72 hours.
When I replaced the acrylic in my Mizuno-type calorimeter with rigid insulation the settling time dropped from 1.6 hours to less than 1/2 hour. Small heat changes (10 W lamp on/off) take only about 8 seconds to appear in the temperature trace.
Mizuno had a bit of built-in delay in his calorimeter response because his reactors are so heavy, (in addition to the bulky acrylic box) to heat.