Well, a lot of good ideas, and suggestions. Thanks. I think I will consider to cut the filler a bit to allow for a larger volume. Of course, I could lower the mass of LAH, but that would mean lowering total mass as well, as I do not want to departure to far away from the 1:10 ratio. (I have done so too much).
With regards to the latest developments with Rossi's patent and the revelations therein, I have ordered Li granules, and gas setup for Argon. Have also found a local supplier of graphite powder for security reasons to keep in the glove box, to quench spontaneous combustion of the Li.
Today I made a new run using a better quality tube, reusing the old coil. The swagelok and transducer seal worked out very well, and at 600 C I had 58 bars. But that is my current headache. I used baked Ni powder, 830mg, 70mg LAH, 50 mg Alumina powder. The Ni was baked 2 hours at ~ 200C. I am seriously concerned that I see no obvious signs of loading in the diagrams. There is still room for it, despite the very high pressure, but I am worried that the Ni powder and LAH is loosing it's pristine qualities, and has become contaminated, loosing the "oomph". The LAH obviously has some go still, otherwise I would not get that excessive pressure. I will power up the reactor Monday and try for excessive heat.
Another concern is that the process need the very rapid temperature and pressure variations that you get from exposing the shell to ambient air, that you don't get with the insulation. It could also be that the current in the coil is too low, failing to give whatever EM kick possibly needed. This I will not address right now because of the effort gone into calibrating the current setup. I will have to stick with the insulated setup for a while longer. One thing that may be explored is the mode of deploying power. I now use manual control of the voltage to set the setpoint temperature, having effectively bypassed the SSR. In my first run, where I had some interesting data, I used the PID controller for the most part, especially, it was used during hydrogenation.
But let's see what happens. I have yet a few experiments to do before giving up