Display MoreOn the contrary - I was assuming nothing other than what you said, which means all I knew was > 5mW.
Now I know "a lot more than 5mW"
I will quantify "a lot" at the lowest value I think is feasible - 2X. And my comments remain.
However, maybe you mean - by "a lot" 10X. or 100X. Who knows?
That (10X) would then mean that I would condition my comments as remaining valid if you had a "typical" electrolysis power of 10W or so. I think 0.5% change in calibration constants for a significant change in experimental conditions is true for many calorimeters. Perhaps not for yours, but testing that is not simple, so without details no-one could assume it had been correctly tested.
So many unknowns. My point is, any scientist, given unknowns, must make no assumptions, and hence be uncertain! But, if these uncertainties can be closed by more transparency and perhaps dealing with a few issues that need to be ruled out, and could easily be ruled out, something unconvincing to mainstream scientists becomes something convincing. Or at least that is my view.
This is, if you like, just a reminder of how mainstream science views these things.
You responded as if what I say here is the only information available and that I need to be reminded that more information must be provided. I said the calorimeter has a sensitivty and uncertainty of ±5 mW. I said nothing about the measured amount and you did not ask. You missed this fact so that you could lecture me on the obvious. Do you realize I have been doing scientific research probably longer than you have been alive and that I know more about the process than you can know? You might consider that you are not lecturing to a college freshman.
The samples are always x10 and sometimes x20 when heated to 500°C. But, we are not debating the accuracy of the data here. I'm trying to have the focus be on the explanation.